Dyeing of Silk with Acid Dyes

This is as per a brochure from CSTRI ( Central Silk Board)

Receipe

M:L- 1:30
Dye- X% on the weight of the material
Glauber Salt- 10% on the weight of the material.
Acetic Acid- 4-6% ( 40% strength)
Temperature: 85-90 deg C, pH-4-6, Time- 15 minutes

Procedure

- Preparation of dye solution: Dissolve required dye powder in boiling water in a separate beaker/vessel.
- Set the dye bath with required quantity of water.
- Add Glauber Salt
- Add dye solution.
- Enter the presoaked material at 40 deg C. Work for 10 minutes.
- Take out the material.
- Add acetic acid and stir well.
- Enter the material.
- Gradually raise the temperature to 85-90 deg C.
- Work for 35-40 minutes
- Take out the material followed by cold wash.
- Removal of excess water by using hydro extractor.
- Dyeing under shade.

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Bleaching and Optical Brightening of Silk

This is as per a brochure from CSTRI ( Central Silk Board)

Bleaching Receipe

M:L- 1:30
Soda Ash- 0.5 GPL or 1% on the weight of the material.
Sodium Silicate- 1.5 GPL
Hydrogen Peroxide- 20 MI/Lit
Temperature- 80 deg C, Time- 60 to 90 Min, pH-9

Procedure
-Take required quantity of water.
-Dissolve soda ash and sodium silicate
- Enter the material at 40 deg C
- Work for 5 min.
- Take out the material and add Hydrogen Peroxide
- Raise the temperature to 80 deg C
-Work for 60-90 min followed by cold wash.
- Removal of excess water by using hydro extractor.

Optical Whitening Receipe

M:L- 1:30
Ranipal WHN-3% on the weight of the material
Hydrose- 2 GPL
Temperature- 60-70 Deg C, Time-15 min, pH-9

Procedure

- Take required quantity of water.
- Add Ranipal WHN and hydrose ( Dissolve Ranipal in hot water)
- Enter the material at 40 deg C.
- Raise the temperature to 60-70 deg C
- Work for 15 minutes followed by cold wash.
- Removal of excess water by using hydro extractor.
- Drying under shade.

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Degumming of Silk

This is as per a brochure from CSTRI ( Central Silk Board)

Receipe

M:L- 1:30
Soap- 5 GPL or 15% on the weight of the material.
Soda Ash- 1 GPL or 3% on the weight of the material
Temperature- 90-95 deg C., Time- 30 to 45 minutes, pH- 9.5 to 10.5

Methods/Procedure

- Dissolve soap and soda in the required amount of water.
- Enter the material at 40 deg C
- Raise the temperature to 90-95 deg C
- Work for 30-45 minutes
- Take out the material and hot wash for 10 minutes for 60 to 70 deg C.
- Followed by cold wash.
- Removal of water by using hydroextractor.
- Drying under Shade.

Single Bath Degumming and Bleaching

Receipe

M:L- 1:30
Soap- 5 GPL or 15% on the weight of the material.
Soda Ash- 0.5 GPL or 1% on the weight of the material.
Sodium Silicate- 1.5 GPL
Hydrogen Peroxide- 20 MI/Lit
Temperature - 85-90 deg C, Time- 60 to90 min., pH- 10

Procedure

- Take required quantity of water.
- Dissolve Soap, Soda Ash and Sodium Silicate
- Enter the material at 40 Deg C
- Work for 5 minutes
- Take out the material and add hydrogen peroxide.
- Raise the temperature to 85-90 deg C
- Work for 60 to 90 minutes followed by hot wash and cold wash.
- Removal of excess water by using hydro extractor.
- Drying in Shade

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Dyeing of Silk with Reactive Dyes

This is as per a brochure from CSTRI ( Central Silk Board Bangalore)

Receipe

M:L- 1:30
Dye: X% on the weight of material.
Glauber Salt- 20% of the weight of material ( 1st Stage)
Glauber Salt- 20% of the weight of material (2nd Stage)
Soda Ash- 5% of the weight of material ( 1st Stage)
Soda Ash- 5% on the weight of material (2nd Stage)
Temperature ( Cold Brand)- 50 deg C
Temperature ( Hot Brand) - 60 deg C
pH-9,  Time: 65-75 minutes

 Procedure

Preparation of dye solution:

Dissolve required dye powder in boiling water in a separate beaker/vessel.

Set the dye bath with required quantity of water.
Add dye solution and add 20% Glauber salt and 5% soda ash at 1st stage.
Enter the material and work for 10 minutes.
Add 20% glauber salt and 5% sold ash at 2nd stage and work for 20 minutes.
For Cold brand reactive dyes, work for 45 minutes at 50 deg.
For hot brand reactive dyes, work for 45 minutes at 60 deg.
Take out the material followed by cold wash.
Remove excess water by using hydro extractor.
Dry under shade.


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